of days let nature take its course,
it does make pretty crystals. Scrape all your crystals up when they are dry put into aher clean pyrex
step 5: Now pour Toluene, about double your psuedo volume **dry/anhydrous**use your epsoms!** over
your powdered psuedo, heat till just befe boiling with your fan blowing over it.
Boil f 5 mins then filter. Repeat this with fresh toluene until when you boil toluene it stays clear. To be
sure of toluene doing its job, after filtering, add water to toluene befe discarding you'll see the *censored*
step 6: Next you can do an acetone wash, by putting your psuedo some acetone in a jar, shake
filter. Dry pseudo you should have *censored*in clean pseudo HCl......
You may choose to react your psuedo now.
Or do an A/B acid/base extraction, basicly turn it into a freebase, oil.
keep in mind..If you do an A/B now, you may lose some psuedo to the povidone.
So what are the choices? well, povidone is known to go thru Hi/RP, no problem, but must be steam distilled
out after. which is a good thing coz you got no seperations emulsions the cleanest meth around.
Povidone is bad because povidone is known to absb hold amines. It depends on what reaction your
4: A/B: Ok, get your nice dry white powder add about equal part water.
Now make up a 20% NaOH solution 4 parts DH2O:1 part NaOH.
Add Toluene to water/pseudo solution about equal to water volume.
Yes, toluene first, it gives the pseudo somewhere to go instead of being burned by the base which can break
it up turn it into aziradines!toxic!
Add NaOH solution to water/pseudo/toluene solution till PH 13, remember to test PH of water toluene!
Now shake the jar up very well let settle into layers.
Seperate toluene layer. Repeat this process 3 times combine all your toluene.
You can wash the toluene/pseudo freebase with water now, if you like, seperate again.
Now you can either, evapate toluene f freebase crystals, you...